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A47656 A course of chemistry containing an easie method of preparing those chymical medicins which are used in physick : with curious remarks and useful discourses upon each preparation, for the benefit of such who desire to be instructed in the knowledge of this art / by Nicholas Lemery, M.D. LĂ©mery, Nicolas, 1645-1715.; Harris, Walter, 1647-1732. 1686 (1686) Wing L1039; ESTC R30931 293,575 606

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neck of one Matrass is put into the neck of another they are called a double vessel and this is done when we desire to circulate Spirits but then the junctures must be very well luted You must also provide many large capacious Recipients for the Distillation of Acid Spirits by a Retort They must be so very large that the Spirits may have room to Circulate the better Lingots are Iron molds of divers shapes into which melted Metals are wont to be poured in order to harden in the form that we would have them That which is used for the making Lapis infernalis must consist of two pieces joined together with two little Iron rings and the melted matter is poured into the upper part of it See its figure in the second Table Coppels are porous vessels made in form of a cup to be used for the trying and purifying of Gold and Silver They are made of Ashes well washt or of bones calcined See their figure in the second Table Ashes deprived of their salts are rather used than others for the composition of this sort of vessels that they may be made the more porous by such deprivation See the Chapter concerning Purification of Silver by the Coppel and the Remarks upon it Many glass Funnels great and small Viols of glass Crucibles Pans Mortars of glass or stone or Marble or Iron must not be forgotten Aludels must also have a place there they are Pots without a bottom joyned together and are placed over another Pot with a whole in the middle to serve for Sublimations Of Lutes The Fire is often raised to so high a degree as will melt glass Retorts in a Reverberatory Furnace wherefore it will be convenient to coat them over with such a Lute as when dry is able to preserve and contain the matter that is put into them to be distill'd This Lute may be made after the manner which follows Take Sand the dross of Iron Potters earth in powder of each five pounds horse-dung cut small a pound glass beaten into powder and Sea-salt of each four ounces mix them all and with a sufficient quantity of water make a Paste or Lute with which you must coat the Retort all round to half its neck and so set it a drying This same Lute will serve to stop close the junctures of the neck of the Retort with the Recipient but because when it dries it grows exceeding hard and it proves difficult to unlute it it is needful to wet it with wet clothes when you would take the Retort asunder from the Receiver The Lute that I commonly use my self for such occasions is compounded only of two parts of Sand and one of clay tempered together with water As for the conjunction of Limbecks ordinary Glue upon paper will serve turn but when something very spirituous is distilled such as the Spirit of Wine use a wet Bladder which carries a Glue along with it that sticks very well But if the bladder happens to be eaten or corroded by the Spirits have recourse to the following Glue Take Flower and Lime slackt of each an ounce Potters-earth in powder half an ounce mix them and make a moist Paste with a sufficient quantity of the Whites of Eggs well beaten before hand with a little water This Paste may likewise serve to stop the cracks that happen in glass vessels there must be three lays of the Paste bound on with paper To Seal Hermetically is to stop the mouth or neck of a Glass-Vessel with a pair of Pincers heated red hot To do this the neck is heated by little and little with burning coals and the fire is encreased and continued until the Glass is ready to melt This way of sealing a Vessel is used when you have put some matter within it that is easie to be exalted and you have a mind to make it Circulate Of the Degrees of Fire To make a Fire of the First Degree two or three coals lighted will suffice to raise a most gentle heat For the Fire of the second degree three or four coals will serve to give such a heat as is able sensibly to warm the Vessel but so as a hand may be able to endure it for some time For the Fire of the Third degree you must cause heat enough to make a Pot boil that is fill'd with five or six quarts of water For the Fourth Degree you must use Coals and Wood together enough to give the most extream heat of all The Fire of Sand of the filings of Iron and of Ashes is made when the Vessel that contains the matter that is to be heated is covered underneath and on all sides with Sand or the filings of Iron or with Ashes this is done to heat the Vessel the more gently All these Fires have their Degrees but the Ash-fire is the mildest because the Ashes cannot contain so great a heat as the others The Reverberatory Fire is made in a close Furnace that the heat or flame which always tends upwards may reverberate or return upon the Vessel which is placed on two Iron bars This fire hath its Degrees but may be raised to a greater violence than the rest The Wheel fire for Fusion is made when with lighted coals you encompass all round a Crucible that holds the matter you desire to melt The Balneum Mariae is when an Alembick containing the matter that is to be heated is placed in a Vessel filled with Water under which the Fire is made thus the water growing hot heats the matter contained in the Alembick The Vaporous Bath is when a Glass vessel containing some Matter is heated by the vapour of hot water Explication of many Terms that are used in Chymistry To Alcoholize or reduce into Alcohol signifies to Subtilize as when a Mixt is beaten into an impalpable powder This word is also used to express a very pure Spirit thus the Spirit of Wine well rectified is called the Alcohol of Wine Amalgamate is to mix Mercury with some melted Metal this Operation serves to render the Metal fit to be extended on some Works as Gold or else to reduce it into a very subtile powder which is done by putting the Amalgame into a Crucible over the Fire for the Mercury subliming into the Air leaves the Metal in an impalpable powder neither Iron nor Copper can by any means be Amalgamated Cement is a manner of purifying Gold 'T is done by stratification with a hard paste made of one part of Salt Armoniack two of common Salt and four of Potters earth or Bricks powdered the whole having been moistned with a sufficient quantity of Urine this Composition is called Royal Cement Circulation is a motion given to liquors contained in a double vessel excited by fire and causing the vapours to ascend and descend to and fro This operation tends either to subtilize the liquors or to open some hard body that is mixed with them Coagulate is to give a consistence to liquids by
as much as lies in my power those things which render it mysterious and dark Spirit of Wine is good for Lethargical and Apoplectical persons because it puts the Spirits into a greater motion than they were in before Now because according to all appearance these Diseases are caused by Obstructions which hinder the course of the Spirits into the Brain this Spirit serves to give them a new vigour to dissolve and rarefie these Tartareous viscosities which shut up their passage It likewise discusses Tumors and Defluxions because it not only opens the pores and gives vent to the subtler part of the humor to perspire but likewise dissolves and rarefies the grosser part so as to render it fit to circulate with the blood The Spirit of Wine is excellent for Burnings provided it be used so soon as they happen for then it opens a passage for the igneous particles to come out at and if there should remain any within the part it unites with them as it uses to do when mixed with an Acid. Spirit of Wine Tartarised This preparation is a Spirit of Wine that has carried with it some portion of Salt of Tartar Put a Pound of Salt of Tartar into a long glass-body pour upon it four pounds of Spirit of Wine prepared as I said before place your vessel in Sand and cover it with a head to which fit a Receiver lute well the junctures with a wet Bladder and give it a gradual fire which continue until three parts of the Spirit of Wine are risen then remove the fire and keep this Spirit in a Viol well stopt it hath the same virtues as the other but is more subtile The liquor that remains in the body may be evaporated and a Salt of Tartar got as good as before Remarks This Operation is only a Rectification of the Spirit of Wine to render it more subtile than it was before because the Salt of Tartar becomes impregnated with the Phlegmatick parts and hinders them from rising The Spirit of Wine doth likewise volatilize and carry along with it some portion of the Salt of Tartar which gives it a very agreeable smell and renders it a good Remedy for Obstructions A sign that the Spirit of Wine has carried along with it some of the Salt of Tartar is this if you dry gently the Salt of Tartar that remains in the Body and weigh it you 'l find it diminished an ounce and a half You may again put this Spirit of Wine Tartarized to half a pound of more Salt of Tartar and distil it as before but I have found that it is never a-whit the better for it This way of Tartarizing Spirit of Wine is the very best and shortest of all that have been invented whether you desire to make it pure or to impregnate it with Salt of Tartar and I may venture to say that all the many long and tedious descriptions that have been given of this Operation have been only invented to cast a dust into the eyes of Novices for it is easie for any to observe who give themselves a little to examine things that after all their long turnings and windings and circumstances to no purpose the Spirit of Wine is not so well Tartarized as by the plain method that I have described Queen of Hungary's Water This Operation is a Spirit of Wine impregnated with the more essential part of Rosemary flowers Fill a glass or earthen cucurbite half full with Rosemary Flowers gathered when they are at their best pour upon it Spirit of Wine sufficient to infuse the Flowers in set your Cucurbite in a Balneum and joyning its head and Receiver lute close the junctures and give it a digesting fire for three days after which unlute them and pour into the Cucurbite that which may have been distilled Refit your Alembick and encrease the fire strong enough to make the liquor distil so as one drop may immediately follow another and when you shall have drawn about two thirds of it and put out the fire let the vessels cool and unlute them you 'l find in the Receiver a very good Water of the Queen of Hungary keep it in a Viol well stopt It is good in the Palsie Lethargy Apoplexy and Hysterical Maladies The Dose is from one drachm to two It is likewise used outwardly for Burnings Tumors Cold pains Contusions Palsie and all other occasions wherein it is requisite to revive the Spirits Ladies do use to mix half an ounce of it with six ounces of Lily-water or Bean-flower water and wash their Face with it to clear their complexion Remarks You must distil this water in a Fire that is strong enough for otherwise the Spirit of Wine would rise alone or else draw along with it but very little Essence as I have observed in the working upon it The Oyl or Essence of Rosemary may be made as the Oyl of Cinnamon and some drops of it mixed in the Spirit of Wine and hereby you have a Queen of Hungary's water made upon the spot The Water of the Queen of Hungary sometimes gives ease to the Tooth-ach being snufft at the Nose or applied to the Gums with a little Cotton Some thinking to Criticize a little do say it is altogether useless to digest Rosemary flowers with Spirit of Wine because their substance being of a very Volatile nature it easily dissolves in the Spirit without any digestion But this Circumstance is very necessary if we desire to have a Water well impregnated with the Essence of the Flowers for although there is a Volatile substance in Rosemary yet good part of the Oil in which consists principally the Smell is involved in the other Principles and cannot be well rarefied mixed and exalted but only by a digestion and thus we have a very good effect from it CHAP. XIII Of Vinegar WInes like all other liquors that use to Ferment do grow sowr by the dissolution of their Tartar in a second Fermentation This dissolution is commonly made when upon the Wines going to decay some of the more subtile Spirits are lost for the Tartar taking their place fixes the rest of the Spirits which remain in the Wine so that they can act no longer This fixation is the cause that when the Wine turns sowr very little quantity of it is diminished and very little Tartar is found in the vessels wherein Vinegar is made To the end that Wine may quickly sowr you must set the Vessel that contains it in some hot place and mix the Lees from time to time for this Tartar will easily dissolve when heat comes to act upon it Perhaps it will be objected that Wine deprived of Tartar and Lees does grow sowr when kept a long time in a vessel without any dissolution of Tartar But we must consider that Wine let it be as clear and pure as may be does always retain the more saline and subtile part of Tartar which exalts and easily smells when by Fermentation it gets the predominancy
marshes When the Season of the year begins to grow hot which commonly happens in May all the water is emptied that was let into the marshes for the better preserving them during the winter then the sluces are opened to let in as much salt-water as they think fit it is made to pass through a great many different Channels wherein it purifies and heats and then is let into places that are made flat smooth and fit to Crystallize the salt The salt is made only during the great heats of Summer the Sun does first evaporate some part of the water and because after the great heat a small wind does use to blow as is usual near the sea the coolness of this wind does condense and Crystallize the salt But if it happens to rain but two hours during the hot weather there can no salt be made for a fortnight afterwards because the marshes must be again emptied of all the water to let in more in its place so that if it chances to rain but once again in the next fortnight they can make no salt Salt is purified by dissolving it in water then filtrating the solution through brown paper and afterwards evaporating the water in an earthen pan until a very white salt does remain But besides the purification of salt by evaporation it may be further purified if instead of evaporation of the humidity you set some of it a Crystallizing in a cool place for very pure salt is found at bottom of the vessel which salt may be separated from the water and dried and you may then evaporate again some part of the salt liquor and set it in a Celler a Crystallizing and so continue your evaporations and Crystallizations but at last you must be fain to evaporate all the liquor because at last it will Crystallize no longer the reason whereof is that the remaining salt is full of a fat bituminous matter which is in a manner inseparable from it and this it is that hinders the Crystallizing at last It is probable that this fat matter may come from the earth of those marshes that were spoken of The first Crystallized salt being put into Oil of Tartar or some other alkali salt dissolved does mix with it without making any Ebullition because although sea salt is acid yet its points are too gross and have too little motion to separate the parts of the alkali The last salt being dried over the fire and mixed with some alkali salt rendred liquid such as Oil of Tartar makes a Coagulation and precipitation of a substance that appears saline and oily this Coagulation does proceed from the mixture and adhesion of some Bituminous earth with the sea-salt and the Tartar for the salts do easily unite with oily substances and in them lose their activity Many acid Bituminous salts which are drawn by the Evaporation of certain Mineral waters such as those of Baleruc in Languedoc and Digne in Provence do perform the same effects when they are mixed with Oil of Tartar This Coagulum does not dissolve in water as well by reason of the different nature of the salts it is compounded of as the oily earth that holds them together but it will dissolve in distilled Vinegar and several other acid liquors and then happens an effervescency because the acid does penetrate the salt of Tartar whose parts the sea-salt had no power to separate Calcination of Common Salt Heat a pot that 's unglazed red-hot throw into it about an ounce of sea-salt then cover it and it will crackle and so fall into powder this noise is called Decrepitation when it is over put so much more salt into the pot and continue to do so till you have enough The pot must be sure to be red-hot all the while when the crackling is over take the pot out of the fire and when it is cold put the salt into a bottle and stop it well to hinder the air from entring in to moisten it anew Bags full of it are applied behind the neck warm to consume too great a a moisture of the Brain by opening of the pores It is used likewise in several Chymical operations Remarks That which makes the Salt crackle when it is in the fire is an inwardly contained moisture which upon its being rarefied doth force its way out with impetuosity and finding the pores too closely shut to suffer an easie escape doth break through the parts and open a passage Now every thing else that hath close compact pores will make such a noise too in the Calcination as do glass and shells If you have occasion to use Salt decrepitated it is convenient to have it newly Calcined because the moisture of the air does return again what the fire had driven away But if you would keep it any time let it be in a glass bottle well stopt For as much as this Salt is deprived of all humidity by its Calcination it will absorb serosities much better than common salt It is laid hot behind the neck to the end that opening the pores it may facilitate transpiration A little Salt of Tartar may be mixed with it to render it the more active Spirit of Salt This Spirit is a very acid liquor drawn from Salt by distillation Dry Salt over a little fire or else in the Sun then powder finely two pounds of it mix it well with six pounds of Potters earth powdered make up a hard paste of this mixture with as much rain-water as is needful form out of it little pellets of the bigness of a Nut and set them in the Sun a good while a drying when they are perfectly dry put them into a large earthen Retort or glass one luted whereof a third part remains empty place this Retort in a Reverberatory Furnace and fit to it a large capacious Receiver without luting the junctures give a very moderate heat at first to warm the Retort and make an insipid water come forth drop by drop when you perceive some white clouds succeed these drops pour out that which is in the Receiver and having refitted it lute the junctures close encrease the fire by degrees to the last degree of all and continue it in this condition twelve or fifteen hours all this while the Receiver will be hot and full of white clouds but when it grows cold and the clouds do disappear the Operation is at an end unlute the junctures and you 'l find the Spirit of Salt in the Receiver pour it into an earthen or glass bottle and stop it well with wax it is an Aperitive and is used in Juleps to an agreeable acidity for such as are subject to the Gravel It is likewise used for cleansing the Teeth being temper'd with a little water and to consume the rottenness of bones To make the dulcified Spirit of Salt of Basilius Valentinus you must mix equal parts of Spirit of Salt and Wine and set them in digestion two or three days in a double Vessel in a